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Brief description
The experimental activities carried out at the MicroChem Lab in Rome focus on the analytical determination of legacy and emerging organic micropollutants and their metabolites, in order to understand their diffusion, distribution, persistence dynamics and fate in the environment. The studies performed at the MicroChem Lab aim also to study the relationships between the climate change and the spread of contaminants at global and local scale. For these purposes, the development and optimization of highly specific and sensitive analytical methodologies for the detection of chemicals at trace and sub-trace concentration levels in the environmental matrices, is required.

Environmental compartments
The experimental activities focus on aquatic and terrestrial ecosystems, therefore the environmental matrices of interest are: Surface waters and sediments (seas, rivers, lakes), snow/ice, soils, aquatic and terrestrial vegetation, biota.

Analytical techniques
The analytical determination of the organic micropollutants is performed by the combination of:
  - Pre-treatment methods (e.g. freeze-drying, filtration, etc.);
  - Extraction/Clean up methods (solid-phase extraction-SPE, pressurized liquid extraction-PLE, liquid-liquid extraction-LL);
  - Sensitive and selective analytical methods based on the coupling of chromatographic techniques (HPLC or GC) with fluorescence, FID-ECD and mass spectrometry detection.

Equipment
The MicroChem Lab is equipped with the following analytical tools:
 
Benchtop lyophilizer (freeze-dryer LABCONCO) 2.5 L capacity, equipped with a touchscreen display, for the pre-treatment of solid matrices subsequently extracted with PLE.
 
Solid Phase Extraction (SPE): 12 inlets solid phase extractor connected to cartridges packed with specific adsorbents for the extraction of target compounds from liquid matrices through a vacuum system.
 
Sonicator (Branson, mod. 2510) for the extraction of chemical compounds from solid matrices by using suitable solvents.
 
ASE 150 (Dionex, Thermo Scientific) to perform pressurized liquid extraction (PLE) of organic pollutants from solid matrices.
 
Speed Extractor E-916 (Buchi) to perform simultaneous pressurized liquid extraction (PLE) of 6 samples, operating in different modes.
 
Rotavapor R 100 (Buchi), equipped with an electronic interface to control the vacuum system and the recirculating chiller.
 
Gas chromatograph (Thermo Fisher, Trace 3000) coupled to mass spectrometry (MS) detector (Thermo Fisher, ISQ7000). The device is connected to an autosampler (Thermo Fisher. AI 1310) and is controlled by a Chromeleon software.
 
HPLC (quaternary pump, column Oven mod. LC-100 and Micro Pump Series 200, Perkin Elmer, USA) coupled to a fluorescence detector (Perkin Elmer Series 200a). The device is controlled by a Chromeleon Software.
 
HPLC (binary pump, Vanquish TM Core HPLC system, Thermo Scientific TM, Italy) coupled to a high-resolution mass spectrometer (Orbitrap Exploris 120, Thermo Scientific TM, Italy). The device is controlled by XcaliburSoftware (version 5.1).
 
Contact person: Dr.Luisa Patrolecco – luisa.patrolecco AT cnr.it

Institute of Polar Science (CNR-ISP)

GIULIANA PANIERI Director

Giuliana Panieri is the new Director of the Institute of Polar Sciences, and her main interests are the study of extreme marine environments and their connections with climate change in the Arctic and elsewhere. For the last 12 years, she has been a full professor of Geology at the Department of Geosciences of the Arctic University of Norway. She has worked at ISMAR CNR (Italy) and at international universities in the USA, Spain, Germany and France. She has served as President of the Biogeosciences Division and Secretary General of the European Geosciences Union (EGU), managing and coordinating numerous national and international projects. Giuliana has published numerous scientific works, has been a book editor, and has been invited several times as a keynote speaker at international conferences. She has led numerous expeditions in the Arctic Oceans. Lately, she has been keen on developing tools for Ocean Literacy and supporting the UN Sustainable Development Goals, implementing specific tasks and deliverables within the framework of numerous national and international projects.
ORCID https://orcid.org/0000-0001-9411-1729    Scopus - Author ID: 56135838100    Loop profile: 835890

E-mail: direttore.isp AT cnr.it
c/o Campus Scientifico - Università Ca' Foscari Venezia
Via Torino, 155
30172 VENEZIA MESTRE (VE)

 

Previous directors:
Mauro Sclavo - Interim Director (From 1st May 2024 until 31st January 2025)
Carlo Barbante (From 1st May 2020 until 30th April 2024)
Leonardo Langone - Interim Director (From 1st June 2019 until 30th April 2020)

Advisory Board

The Institute Advisory Board (Art. 13, Regolamento Organizzazione e Funzionamento CNR del 2019) consists of the Director, who presides over it, six elected representatives of the researchers and technologists of the Institute and one technical-administrative staff representative.
 
The ISP Advisory Board members are:

. . . . . . . .
Giuliana Panieri

 M.Sclavo (until 2024/31/01)
 C.Barbante (until 2024/30/04)
Warren Raymond Lee Cairns
(Representative of the
Researchers and Technologists)
Pamela Cialli
(Representative of the
Technical-Administrative staff)
Fabiana Corami
(Representative of the
Researchers and Technologists)
Francesco Filiciotto
(Representative of the
Researchers and Technologists)
Angelina Lo Giudice
(Representative of the
Researchers and Technologists)
Angelo Lupi
(Representative of the
Researchers and Technologists)
Francesca Spataro
(Representative of the
Researchers and Technologists)

 

Previous Advisory Board
December 21, 2019 - December 19, 2023
Director: Carlo Barbante
Representatives of the researchers and technologists: Maurizio Azzaro, Fabiana Corami, Federico Giglio, Elena Gregoris, Mauro Mazzola, Rosamaria Salvatori
Representative technical-administrative staff: Alessandro Cosenza

The Amundsen-Nobile Climate Change Tower (CCT) is a scientific platform dedicated to studying the thermodynamic characteristics of the atmospheric boundary layer and the exchange processes between the surface and the lower layers of the atmosphere. The structure is composed of 17 modules equipped with patch boxes to provide a power supply and data connection that ends in a dedicated hut at 40 m from the tower, where the acquisition systems are located. The CCT provides continuous profiles of meteorological parameters at four levels up to 34 m, measurements of turbulent fluxes of momentum heat and moisture at two levels as well as of radiation balance components (visible and infrared). Measurement of the characteristics of the snow layer (depth and temperature) are also provided in conjunction with the atmospheric parameters.

Due to the uniqueness of such an infrastructure in Ny-Ålesund, since 2012, the CCT and the surrounding area have become a point of reference for the integrated observation of the components of the climate system. Offering access to national and international research groups, new scientific installations have been set up. In particular for the measurement of greenhouse gases (in collaboration with KOPRI); for the measurement of the snow cover index and spectral reflectivity of the snow; for remote sensing of wind profiles with SODAR and WindLIDAR (in collaboration with KOPRI); to study processes in the active layer, the vegetation, the snow cover and the permafrost temperature profiles.


  - Welcome page with real time data
    

The Institute of Polar Sciences (ISP) of the National Research Council was born on June 1st, 2019 with act n.81 on 31/05/2019 of President Inguscio. The idea of a Polar Institute has its roots in research activities, which have expanded over time, starting from the first years of Antarctic research in 1985. The construction of the Italian base in Antarctica (MZS station) before and the base in the Arctic (DI station) afterwards, has allowed the development of two generations of polar researchers who have made these remote environments their natural laboratory and their home away from home.
 

Vittuari Luca Full Professor within the Class 08/A4 - Geomatics at the University of Bologna Department DICAM. Coordinator of the PhD@DICAM Doctoral course, composed by four curricula (PhD in Civil, Chemical, Environmental and Materials Engineering) of DICAM. Scientific Responsible of the Land Surveying and Geomatics Laboratory (LARIG). Part of the International GNSS Service and member of the University Consortium: UNAVCO.
Main scientific and research activities in the polar regions:
- Researches in Antarctica for the study of geodynamics and for the study of glaciers movements, within the National Program of Research in Antarctica (PNRA) since 1990.
- To date he attended 10 scientific expeditions in Antarctica and one in Arctic (Svalbard Islands) in 2002.
- Responsible of the GPS geodetic network for the study of the ice surface velocity field around the site of the deep ice coring at Dome Concordia (European Project for Ice Core in Antarctica, EPICA).
- Member of the European Project H2020 Beyond EPICA – Oldest Ice, with the aim to retrieve a continuous ice core to bedrock in Antarctica, covering the climate history of the Mid Pleistocene Transition and beyond.
- Responsible of the GNSS permanent station installed at Station Concordia.
- Contribution for the installation and data analysis of a tide gauge station at Italian Mario Zucchelli Station (Antarctica).

Severi Mirko He received his bachelor's degree in Chemistry at the University of Florence in 2000. From 2001 to 2004, in the framework of his PhD at the Department of Chemistry, University of Florence, he worked on the development of semi-continuous ion chromatography coupled to Flow Analysis systems within the European project EPICA (European project for Ice Coring in Antarctica). On 20 April 2004 he got his PhD in Chemical Sciences. He took part in the national research campaigns in Antarctica 2001-2002 and 2003-2004 in the bases of Dome Concordia and Baia Terra Nova running chromatographic analyses in situ on a deep ice core perforated at Dome C as part of the EPICA project.
Since June 2002, he took part to several EPICA-DML and TALDICE ice core processing campaigns at the Alfred Wegener Institute for Polar and Marine Research in Bremerhaven (D). He participated to numerous sampling campaigns in the Arctic (at the Dirigibile Italia base in Ny Alesund) for the study of climate change through the monitoring of atmospheric aerosol. From December 2004 to 31st January 2018 he was the holder of several fellowships and research grants focused on to the development and application of analytical methods on ice cores and climate archives. From 01/02/2018 to 30/11/2018 he was Fixed term Researcher (RTDa) at the "Ugo Schiff" Department of Chemistry of the University of Florence SSD CHIM / 01. Starting from 01/12/2018 he held the position of Tenure track Researcher (RTDb) at the "Ugo Schiff" Department of Chemistry of the University of Florence SSD CHIM / 01. He is associated Professor at University of Florence since 1st December 2021.

Parmiggiani Fiorigi Flavio Degree in Physics from the University of Milan. Retired since 2013, he currently works as an associate researcher at CNR-ISAC where, since 2001, he has been Research Director. Recent research activity has been mainly carried out in the participation in two European projects:
- ICE-ARC
- SPICES
The research topic for which the association with CNR-ISP was requested is the study of the characteristics and distribution of sea ice in polar areas with SAR images.

Gambaro Andrea Full Professor at the Ca’ Foscari University of Venice. Since 2003 he has supervised teaching activities in the Degree Courses in Chemistry, in Chemical Sciences for Conservation and Restoration (SCCR), in Materials Science and Technologies and in Environmental Sciences. His research is focused mainly on: 1) studies on the origin, seasonal evolution and environmental fate of organic sulfur compounds of biological origin (dimethyl sulfide, carbon sulfide and dimethyl sulfonyopropionate) produced in the aquatic system; 2) development of analytical methodologies for the determination of organic micro pollutants (PCB, PAH, PCN, PBDE, PCDD, PCDF, IA) in environmental matrices (water, sediment, atmospheric aerosol) by gas chromatography coupled to both low and high resolution mass spectrometry; 3) development of analytical methodologies for the determination of natural organic compounds (amino acids, sugars, methoxyphenols, algal and fungal toxins, etc.. ) and anthropic (fragrances, aromatic pollutants) in water, biota, aerosol, snow and ice by liquid chromatography coupled with mass spectrometry for the study of local, global contamination and climate change. This activity has led to collaborations with various research groups (Griffith University, Australia; University of Charleston, U.S.A.; Boston College, U.S.A.; University of Sarajevo, Bosnia and Herzegovina; University of Belgrade, Serbia; Aristotle University of Thessaloniki, Greece; University of Rijeka, Croatia; University of Tirana, Albania, etc.. ).
As part of the National Antarctic Research Programme he was responsible for Research Unit (UO) in 2004-2006; Principal Investigator in 2010-2012; responsible of UO in 2013-2014 and since 2016.
The research activity has led to the publication of over 140 publications of which 126 appear on SCOPUS, 10 chapters of books and about 200 communications at national and international conferences (h-index= 30).

Becagli Silvia Graduate in Chemistry and Pharmaceutical Technology in 1991 at the University of Florence, in 1998 Philosophy Doctor in Environmental Science with the thesis Study of Antarctic ecosystem by ice core chemical analysis. Since 1999 she has a permanent position at the Department of Chemistry - University of Florence. In 2013 and 2017 she obtained the National Abilitation for Professor in Analytical Chemistry and in 2017 she obtained the National Abilitation for full Professor in Analytical Chemistry.
Now she works on the application of innovative highly performance analytical methods for the determination of ions and metals in environmental matrices, mainly aerosols, snow and ice. The research activity is focused on the study of the atmospheric aerosol sources and transport processes in areas with different anthropogenic impact, with particular attention to polar areas (Arctic, Antarctica) and marine areas in the central Mediterranean basin. An important part of her research activity is the study of the cycles of natural substances, the anthropogenic contributions and the aerosol-climate interaction for present time, by aerosol measurements, and for the past by chemical analysis of ice cores drilled in Antarctica. She is Editor of the following Journal/issue:
- Special issue jointly organized between Biogeosciences and Atmospheric Chemistry and Physics, Atmospheric deposition in the low-nutrient-low-chlorophyll (LNLC) ocean: effects on marine life today and in the future.
- International Journal Environmental Research and Public Health – Section “Environmental Chemistry and Technology” (IF 2018 = 2.468).
She is author/co-author of 117 and 122 publications from ISI Web of Science and Scopus respectively and she has H-index of 30.

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